2VG3

Rv2361 with citronellyl pyrophosphate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	CCD
Spacegroup name	P 32
Unit cell lengths	86.870, 86.870, 184.070
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	75.160 - 1.800
R-factor	0.204
Rwork	0.203
R-free	0.23100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.264
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	5.000	1.800
High resolution limit [Å]	1.800	1.700
Rmerge	0.070	0.420
Number of reflections	134070
<I/σ(I)>	12	2
Completeness [%]	93.0	92
Redundancy	2.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1