2V06
Crystal structure of the PPM Ser-Thr phosphatase MsPP from Mycobacterium smegmatis at pH 5.5
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-06-03 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 74.718, 83.596, 33.638 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.050 |
| R-factor | 0.1314 |
| R-free | 0.18750 |
| Structure solution method | OTHER |
| RMSD bond length | 0.014 |
| RMSD bond angle | 0.035 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 15.000 | 1.100 |
| High resolution limit [Å] | 1.050 | 1.050 |
| Rmerge | 0.030 | 0.410 |
| Number of reflections | 97914 | |
| <I/σ(I)> | 11.3 | 2.7 |
| Completeness [%] | 98.8 | 99.2 |
| Redundancy | 2.7 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | pH 5.5 |
