2RKU
Structure of PLK1 in complex with BI2536
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 66.593, 66.593, 154.110 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 33.410 - 1.950 |
| R-factor | 0.192 |
| Rwork | 0.190 |
| R-free | 0.24100 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.438 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 2.020 |
| High resolution limit [Å] | 1.950 | 4.200 | 1.950 |
| Rmerge | 0.069 | 0.044 | 0.505 |
| Number of reflections | 29527 | ||
| <I/σ(I)> | 12.7 | ||
| Completeness [%] | 99.9 | 99.1 | 99.9 |
| Redundancy | 6.6 | 6.8 | 6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
