2QYI
Crystal structure of a binary complex between an engineered trypsin inhibitor and Bovine trypsin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-08-16 |
| Detector | MAR scanner 345 mm plate |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 143.694, 77.437, 72.907 |
| Unit cell angles | 90.00, 103.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.600 |
| Rwork | 0.208 |
| R-free | 0.26800 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.544 |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.600 |
| Rmerge | 0.088 |
| Number of reflections | 23234 |
| <I/σ(I)> | 4 |
| Redundancy | 2.91 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 30% Jefamine, VAPOR DIFFUSION, temperature 293K |
