Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-08-05 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.008 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 141.248, 141.248, 211.705 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.080 - 2.700 |
| R-factor | 0.20434 |
| Rwork | 0.202 |
| R-free | 0.25329 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | GGPS1 MONOMER BUILT INTO SAD-PHASED MAP (UNPUBLISHED) |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.389 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.080 | 2.720 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Number of reflections | 59513 | |
| <I/σ(I)> | 12 | 2.83 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 7.7 | 6.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 25% PEG 3350, 0.2M MG FORMATE, pH 5.50, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
