2OY4
Uninhibited human MMP-8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-27 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 |
Unit cell lengths | 33.294, 47.110, 61.325 |
Unit cell angles | 77.73, 80.04, 77.01 |
Refinement procedure
Resolution | 33.170 - 1.700 |
R-factor | 0.23121 |
Rwork | 0.225 |
R-free | 0.29313 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bzs |
RMSD bond length | 0.020 |
RMSD bond angle | 1.614 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.550 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.103 | 0.245 |
Number of reflections | 30329 | |
<I/σ(I)> | 4.7 | 2.6 |
Completeness [%] | 90.3 | 88.3 |
Redundancy | 1.5 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | 0.1M Tris-HCl, 20% PEG3350, 200mM acetohydroxamic acid, 0.2M MgCl2, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |