2OAN
Structure of oxidized beta-actin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-11 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.00000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 119.174, 222.589, 133.719 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.980 - 2.606 |
R-factor | 0.21383 |
Rwork | 0.210 |
R-free | 0.28812 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1j6z |
RMSD bond length | 0.010 |
RMSD bond angle | 1.389 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.980 | 2.680 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.129 | 0.646 |
Number of reflections | 52031 | |
<I/σ(I)> | 9.34 | 1.72 |
Completeness [%] | 94.7 | 76.4 |
Redundancy | 3.6 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 1.6 M (NH4)2SO4, 0.1 M HEPES, 0.1 M NaCl, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |