2NRY
Crystal structure of IRAK-4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 141.502, 139.748, 87.656 |
| Unit cell angles | 90.00, 123.76, 90.00 |
Refinement procedure
| Resolution | 90.000 - 2.150 |
| R-factor | 0.2117 |
| Rwork | 0.209 |
| R-free | 0.26050 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.694 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 90.000 |
| High resolution limit [Å] | 2.130 |
| Number of reflections | 79301 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 6.4 | 293 | 2.6 - 2.9 M ammonium sulfate, PH 6.4-7.9 , EVAPORATION, temperature 293K |
