2JLS

Dengue virus 4 NS3 helicase in complex with ADP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	P 43
Unit cell lengths	52.313, 52.313, 192.932
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.840 - 2.230
R-factor	0.1883
Rwork	0.185
R-free	0.24015
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2jlq
RMSD bond length	0.007
RMSD bond angle	0.981
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.400	2.300
High resolution limit [Å]	2.200	2.200
Rmerge	0.070	0.370
Number of reflections	24904
<I/σ(I)>	21.3	5.3
Completeness [%]	98.3	95
Redundancy	7.1	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1