2JG7
Crystal structure of Seabream Antiquitin and Elucidation of its substrate specificity
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS |
| Synchrotron site | PAL/PLS |
| Temperature [K] | 100 |
| Spacegroup name | P 1 |
| Unit cell lengths | 88.160, 111.020, 113.640 |
| Unit cell angles | 90.50, 98.10, 111.59 |
Refinement procedure
| Resolution | 30.190 - 2.830 |
| R-factor | 0.211 |
| Rwork | 0.210 |
| R-free | 0.22800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bpw |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.062 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.200 | 2.900 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.120 | 0.300 |
| Number of reflections | 86382 | |
| <I/σ(I)> | 7.3 | 2.1 |
| Completeness [%] | 93.0 | 85 |
| Redundancy | 2.9 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
