2JDT
Structure of PKA-PKB chimera complexed with ISOQUINOLINE-5-SULFONIC ACID (2-(2-(4-CHLOROBENZYLOXY) ETHYLAMINO)ETHYL)AMIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.863, 75.563, 80.097 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.880 - 2.150 |
R-factor | 0.203 |
Rwork | 0.200 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yds |
RMSD bond length | 0.013 |
RMSD bond angle | 1.342 |
Refinement software | REFMAC (5.2.0019F) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.900 | 2.230 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.080 | 0.360 |
Number of reflections | 23262 | |
<I/σ(I)> | 8.5 | 2.6 |
Completeness [%] | 99.0 | 100 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |