2J0G

L-ficolin complexed to N-acetyl-mannosamine

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	CCD
Collection date	2005-04-21
Detector	ADSC CCD
Spacegroup name	P 32
Unit cell lengths	96.940, 96.940, 139.470
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	15.000 - 2.850
R-factor	0.196
Rwork	0.193
R-free	0.24800
Structure solution method	OTHER
RMSD bond length	0.011
RMSD bond angle	1.394
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.800
Rmerge	0.080
Number of reflections	33923
<I/σ(I)>	11.6
Completeness [%]	97.6
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1