2IYP
product rup
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-05-17 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 71.062, 105.061, 240.484 |
Unit cell angles | 90.00, 98.26, 90.00 |
Refinement procedure
Resolution | 29.810 - 2.790 |
R-factor | 0.182 |
Rwork | 0.179 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.307 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.080 | 0.250 |
Number of reflections | 39483 | |
<I/σ(I)> | 6.5 | 3 |
Completeness [%] | 90.7 | 81.9 |
Redundancy | 1.8 | 1.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.2 | 25% PEG 3350, 0.1M SODIUM CACODYLATE, 300MM AMMONIUM ACETATE, pH 7.20 |