2IX6
SHORT CHAIN SPECIFIC ACYL-COA OXIDASE FROM ARABIDOPSIS THALIANA, ACX4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-02-12 |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 198.600, 198.600, 150.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 171.500 - 3.900 |
R-factor | 0.247 |
Rwork | 0.247 |
R-free | 0.25100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ix5 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.880 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 4.100 |
High resolution limit [Å] | 3.900 | 3.900 |
Rmerge | 0.150 | 0.320 |
Number of reflections | 27647 | |
<I/σ(I)> | 7.4 | 2 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 9.2 | 9.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.1 M BIS-TRIS-PROPANE PH 7.0, 6% PEG8000, 8% GLYCEROL |