2GWF
Structure of a USP8-NRDP1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-01-21 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9800 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.111, 67.094, 99.275 |
Unit cell angles | 90.00, 91.12, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.300 |
R-factor | 0.20767 |
Rwork | 0.206 |
R-free | 0.23704 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.191 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 41906 | |
<I/σ(I)> | 21.98 | 3.15 |
Completeness [%] | 93.4 | 97.8 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 12% PEG5000 MME, 0.1 M bis-Tris, 1 mM DTT, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |