2FVZ
Human Inositol Monophosphosphatase 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I911-5 |
| Synchrotron site | MAX II |
| Beamline | I911-5 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-12-04 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9075 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 65.030, 96.950, 106.970 |
| Unit cell angles | 90.00, 90.03, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.400 |
| R-factor | 0.2141 |
| Rwork | 0.211 |
| R-free | 0.29740 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.021 |
| RMSD bond angle | 0.021 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | SHELX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.500 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Number of reflections | 51914 | |
| <I/σ(I)> | 16.85 | 3.2 |
| Completeness [%] | 99.8 | 99.8 |
| Redundancy | 3.8 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 298 | 20% PEG 6000, 0.1M Hepes pH 6.8, 0.2M NaCl, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
