2C0C
Structure of the MGC45594 gene product
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-08-05 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 61.164, 82.137, 73.905 |
| Unit cell angles | 90.00, 112.54, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.450 |
| R-factor | 0.166 |
| Rwork | 0.163 |
| R-free | 0.21600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1qor |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.764 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.500 | 1.550 |
| High resolution limit [Å] | 1.450 | 1.450 |
| Rmerge | 0.110 | 0.540 |
| Number of reflections | 116573 | |
| <I/σ(I)> | 11.24 | 2.27 |
| Completeness [%] | 97.7 | 96.1 |
| Redundancy | 4.89 | 3.18 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 9.1 | 0.1 M BICINE PH=9.1 24% PEG 10K, pH 9.10 |
