2BA0
Archaeal exosome core
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 101.570, 129.590, 102.330 |
Unit cell angles | 90.00, 101.56, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.700 |
Rwork | 0.216 |
R-free | 0.26400 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.380 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELXS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 69958 | |
Completeness [%] | 98.1 | 84.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293.15 | 0.1M HEPES, 35% MPD, 10mM CaCl2, 15% Glycerol, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293.15 | 0.1M HEPES, 35% MPD, 10mM CaCl2, 15% Glycerol, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |