2ATI

Glycogen Phosphorylase Inhibitors

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Spacegroup name	P 31
Unit cell lengths	124.500, 124.500, 123.200
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	? - 1.900
R-factor	0.234
Rwork	0.232
R-free	0.25600
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	MOSFLM
Data scaling software	XDS
Phasing software	AMoRE
Refinement software	CNX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	500.000	2.000
High resolution limit [Å]	1.900	1.900
Number of reflections	167664
Completeness [%]	99.6	100

Crystallization Conditions

crystal ID	method	pH	temperature	details
1