2ABZ
Crystal structure of C19A/C43A mutant of leech carboxypeptidase inhibitor in complex with bovine carboxypeptidase A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Collection date | 2004-06-21 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 124.930, 124.930, 154.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.160 |
R-factor | 0.19 |
Rwork | 0.189 |
R-free | 0.23400 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | REFMAC (5.1.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.100 |
Number of reflections | 66322 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 1.5M Lithium Sulfate monohydrate, 100mM Tris, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |