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1ZT5

C-terminal domain of Insulin-like Growth Factor Binding Protein-1 isolated from human amniotic fluid complexed with Iron(II)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsELETTRA BEAMLINE 5.2R
Synchrotron siteELETTRA
Beamline5.2R
Temperature [K]100
Detector technologyCCD
Collection date2004-01-14
DetectorMARRESEARCH
Wavelength(s)1.0
Spacegroup nameP 21 21 2
Unit cell lengths38.210, 59.600, 31.060
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution22.340 - 1.818
R-factor0.22333
Rwork0.222
R-free0.26425
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.008
RMSD bond angle1.421
Data reduction softwareMOSFLM
Data scaling softwareCCP4 ((SCALA))
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]22.3401.880
High resolution limit [Å]1.8181.818
Number of reflections6773
<I/σ(I)>8.95.6
Completeness [%]97.098.3
Redundancy3.48
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.5277dioxane, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K

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