1ZGL

Crystal structure of 3A6 TCR bound to MBP/HLA-DR2a

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	2004-10-01
Detector	SIEMENS HI-STAR
Wavelength(s)	1.5418
Spacegroup name	P 1
Unit cell lengths	96.480, 97.690, 124.020
Unit cell angles	74.39, 83.19, 61.55

Refinement procedure

Resolution	30.000 - 2.800
Rwork	0.280
R-free	0.32900
Structure solution method	MOLECULAR REPLACEMENT
Phasing software	AMoRE
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.920
High resolution limit [Å]	2.800	2.800
Rmerge	0.080	0.284
Number of reflections	81551
<I/σ(I)>		2.5
Completeness [%]	0.9	86.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1