1Z1A
S. cerevisiae Sir1 ORC-interaction domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-ID-B |
Synchrotron site | APS |
Beamline | 14-ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-11-22 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9793, 0.9795, 0.9688 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 60.928, 60.928, 159.257 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.500 |
R-factor | 0.24148 |
Rwork | 0.238 |
R-free | 0.27424 |
Structure solution method | MAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.012 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 11994 | |
Completeness [%] | 98.3 | 91.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | sodium acetate, PEG 400, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |