1YP2

Crystal structure of potato tuber ADP-glucose pyrophosphorylase

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-BM
Synchrotron site	APS
Beamline	19-BM
Temperature [K]	100
Detector technology	CCD
Collection date	2003-03-17
Detector	CUSTOM-MADE
Wavelength(s)	1.00739, 1.00922, 0.99298
Spacegroup name	P 1 21 1
Unit cell lengths	79.465, 137.551, 91.623
Unit cell angles	90.00, 112.53, 90.00

Refinement procedure

Resolution	19.940 - 2.110
R-factor	0.172
Rwork	0.172
R-free	0.22900
Structure solution method	MAD
RMSD bond length	0.011
RMSD bond angle	1.600
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.230
High resolution limit [Å]	2.100	2.100
Number of reflections	84060
Completeness [%]	80.2	99.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1