1YBK
RHCC cocrystallized with CAPB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ELLIOTT GX-20 |
| Detector technology | IMAGE PLATE |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 110.811, 110.811, 71.121 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 6.000 - 1.450 |
| R-factor | 0.211 |
| Rwork | 0.211 |
| R-free | 0.22600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.700 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 1.490 | |
| High resolution limit [Å] | 1.400 | 1.400 |
| Number of reflections | 86287 | |
| <I/σ(I)> | 14.6 | 2.7 |
| Completeness [%] | 96.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.9 | 273 | ammonium sulfate, pH 7.9, VAPOR DIFFUSION, HANGING DROP, temperature 273K |
