1Y0H
Structure of Rv0793 from Mycobacterium tuberculosis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-09-13 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.979232 |
Spacegroup name | P 1 |
Unit cell lengths | 30.440, 34.600, 42.850 |
Unit cell angles | 103.44, 107.96, 94.34 |
Refinement procedure
Resolution | 29.590 - 1.600 |
R-factor | 0.202 |
Rwork | 0.173 |
R-free | 0.21900 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.219 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE (2.06) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.098 | 0.485 |
Number of reflections | 20461 | |
<I/σ(I)> | 8.5 | 4.8 |
Completeness [%] | 96.9 | 95.4 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | PEG20K, hepes, ammonium acetate, ethylene glycol, isopropanol, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |