1XZ1
Complex of halothane with apoferritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-03-04 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9197 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.610, 181.610, 181.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.750 |
R-factor | 0.181 |
Rwork | 0.179 |
R-free | 0.21157 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1gwg |
RMSD bond length | 0.011 |
RMSD bond angle | 1.187 |
Data scaling software | d*TREK |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.820 |
High resolution limit [Å] | 1.710 | 1.710 |
Rmerge | 0.081 | 0.514 |
Number of reflections | 28090 | |
<I/σ(I)> | 15.9 | 3.7 |
Completeness [%] | 99.5 | 99.2 |
Redundancy | 18.2 | 8.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | cadmium sulfate, HEPES, sodium acetate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |