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Structure of human Dcps
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2004-07-14 |
| Detector | MACSCIENCE DIP100 |
| Wavelength(s) | 0.93 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 101.922, 103.863, 71.067 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.000 |
| R-factor | 0.22108 |
| Rwork | 0.220 |
| R-free | 0.25259 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.142 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.500 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 51155 | |
| Completeness [%] | 98.9 | 90 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.4 | 298 | KH2PO4, NaCl, PEG3350, pH 4.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
