1XKP
Crystal structure of the virulence factor YopN in complex with its heterodimeric chaperone SycN-YscB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Collection date | 2003-11-25 |
Spacegroup name | P 41 |
Unit cell lengths | 60.718, 60.718, 140.419 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.860 - 1.700 |
R-factor | 0.20059 |
Rwork | 0.198 |
R-free | 0.24197 |
Structure solution method | MIR |
RMSD bond length | 0.013 |
RMSD bond angle | 1.494 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.860 |
High resolution limit [Å] | 1.700 |
Number of reflections | 55724 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |