Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X9A |
| Synchrotron site | NSLS |
| Beamline | X9A |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2001-05-27 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9794, 0.9792, 0.9648 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 189.240, 88.970, 112.910 |
| Unit cell angles | 90.00, 106.09, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.900 |
| R-factor | 0.232 |
| Rwork | 0.228 |
| R-free | 0.27600 |
| Structure solution method | MAD |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 3.000 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 75343 | |
| Completeness [%] | 96.2 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | CaCl2, PEG 400, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
