1WXE
E.coli NAD Synthetase, AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 92.450, 67.820, 48.282 |
Unit cell angles | 90.00, 104.47, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.900 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.198 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 25734 | |
Completeness [%] | 95.9 | 92.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.2 | 295 | PEG400, magnesium chloride, sodium-acetate, lithium-meta-tantalate, pH 5.2, VAPOR DIFFUSION, temperature 295K |