1WSE
Co-crystal structure of E.coli RNase HI active site mutant (E48A*) with Mn2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Detector technology | CCD |
Collection date | 2004-02-16 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9791 |
Spacegroup name | P 2 2 21 |
Unit cell lengths | 58.041, 66.008, 79.485 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.300 |
Rwork | 0.230 |
R-free | 0.28800 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 13962 | |
Completeness [%] | 98.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |