1WLJ
human ISG20
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32B2 |
Synchrotron site | SPring-8 |
Beamline | BL32B2 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-03-17 |
Detector | RIGAKU RAXIS V |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 63.420, 63.420, 97.910 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
Rwork | 0.207 |
R-free | 0.22700 |
Structure solution method | MAD with data collected at 1.0085, 1.005, 0.92 A |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNX |
Refinement software | CNX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 55.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.039 |
Number of reflections | 18442 |
Completeness [%] | 99.5 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 296 | sodium acetate, sodium chloride, 1-butanol, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 296K |