1WAQ
Crystal structure of human Growth and Differentiation Factor 5 (GDF-5)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-08-16 |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 97.771, 97.771, 43.325 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 17.000 - 2.280 |
R-factor | 0.223 |
Rwork | 0.222 |
R-free | 0.23700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bmp |
RMSD bond length | 0.017 |
RMSD bond angle | 1.412 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.520 | 2.390 |
High resolution limit [Å] | 2.280 | 2.280 |
Rmerge | 0.050 | 0.190 |
Number of reflections | 11084 | |
<I/σ(I)> | 8.7 | 3.4 |
Completeness [%] | 98.3 | 93.3 |
Redundancy | 4.5 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 25% 2-METHLY-2,4-PENTANEDIOL, 0.1M SODIUM CITRATE PH 4.0 |