1WAO
PP5 structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-11-10 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.740, 117.540, 200.410 |
| Unit cell angles | 90.00, 93.79, 90.00 |
Refinement procedure
| Resolution | 33.780 - 2.900 |
| R-factor | 0.247 |
| Rwork | 0.247 |
| R-free | 0.29000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.375 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.110 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.120 | 0.420 |
| Number of reflections | 53119 | |
| <I/σ(I)> | 3.4 | 1.4 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 6.9 | 5.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | PEG 6K 10% |
