1W6S

The high resolution structure of methanol dehydrogenase from methylobacterium extorquens

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	150
Spacegroup name	P 1
Unit cell lengths	62.900, 73.620, 88.080
Unit cell angles	86.09, 104.11, 109.68

Refinement procedure

Resolution	10.000 - 1.200
R-factor	0.1576
R-free	0.17690
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.022
RMSD bond angle	0.046
Refinement software	SHELXL-97

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.230
Rmerge	0.100
Number of reflections	373341
<I/σ(I)>	2.3
Completeness [%]	90.3
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1