1W2K

tf7a_4380 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1996-09-16
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	71.874, 82.638, 123.722
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.820 - 3.000
Rwork	0.197
R-free	0.25700
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1w0y
RMSD bond length	0.006
RMSD bond angle	1.400
Data reduction software	XDS
Data scaling software	XDS
Refinement software	CNX (2002)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.870	3.200
High resolution limit [Å]	3.000	3.000
Rmerge	0.160	0.290
Number of reflections	14546
<I/σ(I)>	12.15	5.02
Completeness [%]	95.0	92.8
Redundancy	3.45	3.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5.5		pH 5.50