1W0Y

tf7a_3771 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM1A
Synchrotron site	ESRF
Beamline	BM1A
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1997-01-30
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	71.338, 82.378, 123.963
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.990 - 2.500
Rwork	0.199
R-free	0.25800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1dan
RMSD bond length	0.010
RMSD bond angle	1.700
Data reduction software	XDS
Data scaling software	XDS
Phasing software	AMoRE
Refinement software	CNX (2002)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.000	2.580
High resolution limit [Å]	2.460	2.460
Rmerge	0.130	0.390
Number of reflections	85076
Completeness [%]	87.8	50.3
Redundancy	3.27	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5.5		pH 5.50