1VTL
CO-CRYSTAL STRUCTURE OF TBP RECOGNIZING THE MINOR GROOVE OF A TATA ELEMENT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 123 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.800, 146.500, 57.600 |
Unit cell angles | 90.00, 90.60, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.250 |
R-factor | 0.202 |
Rwork | 0.202 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.600 |
Number of reflections | 18312 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.2 | 277 | pH 6.20, VAPOR DIFFUSION, temperature 277.00K |
1 | VAPOR DIFFUSION | 6.2 | 277 | pH 6.20, VAPOR DIFFUSION, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | 2 | 3 |
10 | 1 | 2 | MES | 29 | 30 |
2 | 1 | 1 | DTT | 5 | 6 |
3 | 1 | 1 | GLYCEROL | 8 | 9 |
4 | 1 | 1 | MES | 11 | 12 |
5 | 1 | 1 | KCL | 14 | 15 |
6 | 1 | 1 | NH4 ACETATE | 17 | 18 |
7 | 1 | 2 | WATER | 20 | 21 |
8 | 1 | 2 | DTT | 23 | 24 |
9 | 1 | 2 | GLYCEROL | 26 | 27 |