Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2002-09-10 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.420, 51.000, 104.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.212 |
Rwork | 0.171 |
R-free | 0.20900 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.680 |
RMSD bond angle | 1.700 |
Data reduction software | bioteX |
Data scaling software | d*TREK (7.2SSIbeta) |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.620 | 1.800 |
High resolution limit [Å] | 1.730 | 1.730 |
Number of reflections | 16006 | |
Completeness [%] | 71.6 | 10.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | Mg formate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |