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1VOL

TFIIB (HUMAN CORE DOMAIN)/TBP (A.THALIANA)/TATA ELEMENT TERNARY COMPLEX

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Temperature [K]123
Detector technologyIMAGE PLATE
DetectorRIGAKU
Spacegroup nameP 21 21 21
Unit cell lengths69.900, 78.000, 134.700
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution8.000 - 2.700
R-factor0.215
Rwork0.215
R-free0.31800
RMSD bond length0.014
RMSD bond angle1.860
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareX-PLOR
Data quality characteristics
 Overall
High resolution limit [Å]2.700
Rmerge0.072

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Total number of observations180515

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Number of reflections20995
Completeness [%]82.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

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8.5

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4

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Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropDNA complex0.3-0.4 (mM)
101reservoirglycerol5-10 (%(v/v))
111reservoirdithiothreitol20 (mM)
121reservoirTris-HCl40 (mM)
131dropethylene glycerol2 (%(v/v))
21drop40 (mM)
31dropammonium acetate300 (mM)
41drop5 (mM)
51drop5 (mM)
61dropzinc acetate0.01 (mM)
71dropdithiothreitol10 (mM)
81dropglycerol10 (%(v/v))
91dropTris-HCl40 (mM)

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PDB entries from 2024-03-27

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