1VLK
STRUCTURE OF VIRAL INTERLEUKIN-10
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1996-05-04 |
Detector | RIGAKU |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 36.270, 36.270, 219.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.900 |
R-factor | 0.191 * |
Rwork | 0.191 |
RMSD bond length | 0.014 |
RMSD bond angle | 0.052 |
Data reduction software | DENZO |
Refinement software | PROFFT |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 1.900 * | 1.900 * |
Rmerge | 0.081 | |
Number of reflections | 9860 | |
Completeness [%] | 82.0 | 47 * |
Redundancy | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 8 (mg/ml) | |
2 | 1 | drop | PEG4000 | 3.4 (mg/ml) | |
3 | 1 | drop | sodium acetate | 0.02 (M) | |
4 | 1 | drop | ammonium sulfate | 0.04 (M) | |
5 | 1 | reservoir | PEG4000 | 14 (%) | |
6 | 1 | reservoir | sodium acetate | 0.1 (M) | |
7 | 1 | reservoir | ammonium sulfate | 0.2 (M) |