Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X8C |
| Synchrotron site | NSLS |
| Beamline | X8C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1999-01-01 |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 89.210, 117.330, 97.480 |
| Unit cell angles | 90.00, 115.09, 90.00 |
Refinement procedure
| Resolution | 19.930 - 2.900 |
| R-factor | 0.232 |
| Rwork | 0.232 |
| R-free | 0.29300 |
| Structure solution method | MAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.500 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 3.080 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 36056 | |
| Completeness [%] | 69.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 295 | 5% methoxyPEG 5000, 100mM sodium citrate(pH 5.6), 5mM calcium chloride, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
