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1V7Z

creatininase-product complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron sitePhoton Factory
BeamlineAR-NW12A
Temperature [K]100
Detector technologyCCD
Collection date2003-10-25
DetectorADSC QUANTUM 210
Wavelength(s)0.9780
Spacegroup nameP 21 21 21
Unit cell lengths102.186, 152.211, 167.119
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 1.600
R-factor0.18288
Rwork0.182
R-free0.19776
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.052
Data reduction softwareMOSFLM
Data scaling softwareCCP4 ((SCALA))
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0001.690
High resolution limit [Å]1.6001.600
Number of reflections333996
<I/σ(I)>13.52
Completeness [%]98.093.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5293litium sulfate, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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