1V55

Bovine heart cytochrome c oxidase at the fully reduced state

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Spacegroup name	P 21 21 21
Unit cell lengths	183.060, 206.584, 178.298
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 1.900
Rwork	0.203
R-free	0.23000
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013 *
RMSD bond angle	1.850 *
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	200.000 *
High resolution limit [Å]	1.900 *	1.900 *
Rmerge	0.092 *	0.318 *
Total number of observations	2806708 *
Number of reflections	522643 *	50069 *
Completeness [%]	98.6 *	95.3 *
Redundancy	5.4 *	3.4 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *			Yoshikawa, S., (1998) Science, 280, 1723. *