1V0E

Endosialidase of Bacteriophage K1F

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE BW7A
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	BW7A
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 2 2 21
Unit cell lengths	99.650, 131.250, 346.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.900
R-factor	0.16781
Rwork	0.166
R-free	0.20228
Structure solution method	MAD
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.900
Rmerge	0.103	0.352
Number of reflections	335241
Completeness [%]	93.7	96
Redundancy	4.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.50