1UZN
MabA from Mycobacterium tuberculosis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-08-15 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 81.539, 117.111, 51.869 |
Unit cell angles | 90.00, 122.62, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.910 |
R-factor | 0.187 |
Rwork | 0.185 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.182 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.960 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.052 | 0.150 |
Number of reflections | 28001 | |
<I/σ(I)> | 17 | 4.3 |
Completeness [%] | 93.1 | 76.2 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.6 | PIPES PH 6.6 CSCL 400 MM, PEG 3000 12%, NADP 100 MM |