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1UYH

Human Hsp90-alpha with 9-Butyl-8-(2,5-dimethoxy-benzyl)-2-fluoro-9H-purin-6-ylamine

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2002-09-15
DetectorRIGAKU RAXIS IV
Spacegroup nameI 2 2 2
Unit cell lengths66.502, 90.414, 98.664
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution65.940 - 2.200
R-factor0.267
Rwork0.264
R-free0.32600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1yer
RMSD bond length0.019
RMSD bond angle1.781
Data reduction softwared*TREK
Data scaling softwared*TREK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.1.19)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.300
High resolution limit [Å]2.2002.200
Rmerge0.0530.311
Number of reflections14468
<I/σ(I)>91.9
Completeness [%]93.691.7
Redundancy4.13.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
16.525% PEG MME 2000, 0.1M NA CACODYLATE, PH6.5, 0.2M MGCL2., pH 6.50

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