1UHL
Crystal structure of the LXRalfa-RXRbeta LBD heterodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-09-02 |
Detector | MARRESEARCH |
Wavelength(s) | 1.11 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.634, 88.996, 90.795 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.650 - 2.900 |
R-factor | 0.2239 |
Rwork | 0.219 |
R-free | 0.32649 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dkf |
RMSD bond length | 0.029 |
RMSD bond angle | 2.776 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.650 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 12550 | |
<I/σ(I)> | 9.2 | 1.9 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 305 | MES, PEG, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 305K |