1UEA
MMP-3/TIMP-1 COMPLEX
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
| Synchrotron site | MPG/DESY, HAMBURG |
| Beamline | BW6 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.979, 1.279 |
| Spacegroup name | P 43 |
| Unit cell lengths | 80.620, 80.620, 157.620 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 100.000 - 2.800 |
| R-factor | 0.197 |
| Rwork | 0.197 |
| R-free | 0.29700 * |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.600 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.750 |
| High resolution limit [Å] | 2.790 |
| Rmerge | 0.110 |
| Number of reflections | 24252 |
| Completeness [%] | 99.6 |
| Redundancy | 14.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, sitting drop * | 6 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | 2.5 (M) | ||
| 2 | 1 | reservoir | epsilon-aminocaproic acid | 200 (mM) | |
| 3 | 1 | reservoir | Tris-HCl | 20 (mM) | |
| 4 | 1 | reservoir | 4 (mM) | ||
| 5 | 1 | reservoir | sodium acetate | 100 (mM) |
